FOOD SCIENCE ›› 2017, Vol. 38 ›› Issue (24): 224-228.doi: 10.7506/spkx1002-6630-201724036
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ZHU Wei, NING Xiaojun, DU Ruyun
Online:
Published:
Abstract: A method was established using high performance ion chromatography and pulsed amperometric detection for simultaneous analysis of 1-kestose (GF2), nystose (GF3), 1F-fructofuranosyl nystose (GF4), GF5, GF6, raffinose, stachyose and verbascose in infant formula milk powder. The chromatographic separation was achieved on a CarboPac PA20 column using a mobile phase composed of a mixture of sodium hydroxide and sodium acetate by gradient elution. Under the conditions optimized in this study, all the analytes were well separated, and the recoveries were 80.0%–103% with a relative standard deviation (RSD) less than 3% (n = 6). The method was rapid, accurate, reliable, and thus suitable for the determination of functional oligosaccharides in infant formula milk powder.
Key words: formula milk powder, functional oligosaccharides, high performance ion chromatography, pulsed amperometric detector
CLC Number:
O657.7
ZHU Wei, NING Xiaojun, DU Ruyun. Determination of Functional Oligosaccharides in Infant Formula Milk Powder by High Performance Ion Chromatography[J]. FOOD SCIENCE, 2017, 38(24): 224-228.
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URL: https://www.spkx.net.cn/EN/10.7506/spkx1002-6630-201724036
https://www.spkx.net.cn/EN/Y2017/V38/I24/224