超临界CO2萃取沙棘籽油及热敏性物质分析

doi:10.7506/spkx1002-6630-201224020

食品科学 ›› 2012, Vol. 33 ›› Issue (24): 97-100.doi: 10.7506/spkx1002-6630-201224020

超临界CO2萃取沙棘籽油及热敏性物质分析

魏贞伟1，邵弘2，王俊国1，王喜权2，胡立志2,*

1.吉林工商学院生物工程分院，吉林长春 130062；2.东北农业大学国家大豆工程技术研究中心，黑龙江哈尔滨 150030

收稿日期:2012-05-10 修回日期:2012-10-24 出版日期:2012-12-25 发布日期:2012-12-12
通讯作者: 于殿宇 E-mail:dyyu2000@yahoo.com.cn
基金资助:
黑龙江省教育厅科学技术研究项目

Supercritical Carbon Dioxide Extraction of Seabuckthorn Seed Oil and Analysis of Thermosensitive Substances

WEI Zhen-wei1，SHAO Hong2，WANG Jun-guo1，WANG Xi-quan2，HU Li-zhi2,*

1. Branch of Biological Engineering, Jilin Business and Technology College, Changchun 130062, China；2. National Research Center of soybean Engineering and Technology, Northeast Agricultural University, Harbin 150030, China

Received:2012-05-10 Revised:2012-10-24 Online:2012-12-25 Published:2012-12-12

摘要/Abstract

摘要：

对超临界CO2萃取沙棘籽油及热敏性物质进行分析研究。通过正交试验确定最佳工艺条件：萃取压力25MPa、萃取温度40℃、CO2流量18kg/h、萃取时间120min、分离压力8MPa，在此工艺条件下沙棘籽油出油率为52%。高效液相色谱法检测沙棘籽油中α-VE含量为2.6%，经超临界CO2萃取后热敏性物质α-VE损失3.7%，胡萝卜素含量为100850μg/100g。

关键词: 超临界CO2, 沙棘籽油, α-VE, 胡萝卜素

Abstract:

In the present study, the supercritical carbon dioxide extraction of seabuckthron seed oil was optimized using an orthogonal array design. Besides, thermosensitive substances in seabuckthron seed oil were analyzed. The optimum extraction conditions were determined as extraction at 40 ℃ at an extraction pressure of 25 MPa and a separation pressure of 8 MPa for 120 min with a CO2 flow rate of 18 kg/h. Under these conditions, the oil yield was 52%. The content of α-VE as a thermosensitive substance in seabuckthron seed oil was 2.6% as determined by HPLC and supercritical carbon dioxide extraction resulted in a 3.7% α-VE loss when compared with cold pressing. The content of carotene in seed oil obtained by supercritical carbon dioxide extraction was 100850 μg/100 g.

Key words: supercritical carbon dioxide, seabuckthorn seed oil, α-VE, carotene

中图分类号:

TS229

魏贞伟1，邵弘2，王俊国1，王喜权2，胡立志2,*. 超临界CO2萃取沙棘籽油及热敏性物质分析[J]. 食品科学, 2012, 33(24): 97-100.

参考文献

[1]银建中,孙献文,原华山,丁信伟.超临界CO2流体萃取沙棘油实验研究[J].化学工业与工程技术,2001, 26(6):9-11.

[2]忻扭年等.沙棘油的特性及其制油工艺[J].中国油脂,1993:(2):8.

[3]赵元藩.沙棘油的精制及其在化妆品中的应用[J].云南师范大学报,2000,20(2):48-49.

[4]曹志丹.沙棘国内外研究状况的评述[J].中国油脂,1993,(3):3-8.

[5]忻耀年,刘永霞.沙棘油质量控制及品质评定分析研究[J].沙棘,1999,12(4):22-27.

[6]梁爱军,张素华,王巨成.超临界CO2萃取沙棘油工艺研究[J].山西林业科技,2000，(3):22-25.

[7]刘永霞,王晓君.沙棘油中幽醇组分的分析[J].四川棘油科技,1998,(2):51-54.

[8]忻耀年,项东方.沙棘油的气液色谱分析及制油工艺研究[J].沙棘,1995,8(1):27-32.

[9]张素华.CO2超临界萃取沙棘油酸价测定[J].山西林业科技,2001(2):15-17.

[10]Sovova H, Kucera J, Jez J?Rate of the vegetable oil ex-tration with supercritical carbon dioxide —Ⅱ.Extraction of grape oil[J].Chem?Engng Sci?,1994,49:415-420.

[11]Cygnarowicz,Miriam L,Seider,Warren?Design and con-trol of a process to extractβ-carotene with supercritical carbon dioxide[J].Biotechnology Progress, 1990,6(1):82-91.

[12]Cuperus F P, Boswinkel G, Derksen T P?Processing of new oilseed crops - an economic evaluation[J].JAOCS,Journal of the American Oil Chemists’Society, 1996,73(12):1635-1640.

[13]Perrut M,Clavier J Y, Poletto M,Reverchon E?Mathe-matical modeling of sunflower seed extraction by super-critical CO2[J].Industrial & Engineering Chemistry Re-search,1997,36(2):

430-435.

[14]Fullana M,Trabelsi F,Recasens F?Use of neural net computing for statistical and kinetic modelling and simu-lation of supercritical fluid extractors[J].Chemical Engi-neering Science, 1999,54(24):5845-5862.

[15]李桂华.油料油脂检验与分析[M].化学工业出版社,2006,179-181.

超临界CO2萃取沙棘籽油及热敏性物质分析

Supercritical Carbon Dioxide Extraction of Seabuckthorn Seed Oil and Analysis of Thermosensitive Substances

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