食品科学 ›› 2012, Vol. 33 ›› Issue (22): 269-273.

• 分析检测 • 上一篇    下一篇

蒸煮和焙炒整米苦荞茶香气成分分析及生产过程中主要化学成分的去向

隋秀芳1,2,李 祥2,秦礼康1,*,赵 宇1,林 敏1   

  1. 1.贵州大学生命科学学院 2.黔东南州质量技术监督检测所
  • 收稿日期:2011-09-24 修回日期:2012-10-08 出版日期:2012-11-25 发布日期:2012-11-20
  • 通讯作者: 秦礼康 E-mail:likangqin@126.com
  • 基金资助:

    贵州省科技厅农业攻关项目;贵阳市生物重大专项

Analysis of Volatile Aroma Compounds in Steamed and Roasted Whole Tartary Buckwheat Teas and Distribution of Major Chemical Components during the Production Process

  • Received:2011-09-24 Revised:2012-10-08 Online:2012-11-25 Published:2012-11-20
  • Contact: likang qin E-mail:likangqin@126.com

摘要: 为探索焙炒、蒸煮与重组造粒加工工艺对苦荞茶香气和营养成分的影响,跟踪检测3种工艺中各组分主要营养成分的流向分布,并采用固相微萃取结合气质联用技术对苦荞茶产品的挥发性香气成分进行对比分析。结果表明,不同工艺所得产物的营养功效成分存在显著性差异(P<0.05)。按蒸煮米工艺生产苦荞茶,蛋白质主要集中分布在黄粉中,含量为27.51g/100g;还原性糖含量从原料的0.69%降为产品的0.28%;功能性成分总黄酮主要分布在抛光粉和黄粉中,含量分别为4.98%和4.63%;由于总黄酮的流向分布使得苦荞茶成品的含量降为1.38%,按焙炒、造粒工艺生产苦荞茶,其中焙炒荞粒总黄酮仅为1.29%,用富含黄酮(4.56%)的苦荞皮粉重组的含茶荞粒,其总黄酮含量高达6.87%,两者混合后成品品质与风味显著优于按蒸煮米工艺生产的苦荞茶。从挥发性香气物质看,蒸煮米工艺苦荞茶以烷烃和烯类为主,而焙炒工艺苦荞茶则以醛类和烷烃为主,且还富含苯酚、醇类、醚类、酮类和酯类,这是焙炒苦荞茶风味优于蒸煮米苦荞茶的原因。

关键词: 苦荞茶, 香气, 营养, 固相微萃取, 气相色谱-质谱分析

Abstract: The distribution of major chemical components during the production of steamed and roasted whole tartary buckwheat tea samples was tracked to explore the effects of steaming, roasting and reconstructed granulation on the aroma and nutritional components of tartary buckwheat tea. Meanwhile, both tartary buckwheat teas were comparatively analyzed for volatile aroma components by solid-phase microwaveextraction (SPME) coupled with GC-MS. The final products obtained following different procedures showed significant differences in chemical composition (P<0.05). During the production of steamed tartary buckwheat tea, proteins were mainly distributed in the yellow powder at a level of 27.51%, the reducing sugar content of 0.69% in the raw material decreased to 0.28% in the fine product, and total flavonoids were mainly distributed in the polished powder and yellow powder at levels of 4.98% and 4.63%, respectively. As a result, the total flavonoid content of the final product was as low as 1.38% compared with only 1.20% for roasted tartary buckwheat grains. The total flavonoid content of tea-containing reconstructed granules prepared from buckwheat husk powder, rich in flavonoids (4.56%), was as high as 6.87%. Roasted whole tartary buckwheat tea as a mixture of roasted tartary buckwheat grains and tea-containing reconstructed granules had considerably better quality and flavor than its steamed counterpart. The major aroma compounds of steamed tartary buckwheat tea were alkanes and alkenes, while roasted tartary buckwheat tea contained aldehydes and alkanes as major aroma compounds and was also rich in phenols, alcohols, ethers, ketones and esters, which caused better flavor in roast tartary buckwheat tea and than steamed one.

Key words: tartary buckwheat tea, aroma compounds, solid phase microextraction (SPME), GC-MS

中图分类号: