Simultaneous Determination of 8 HCH and DDT Residues in Soybean and Soybean Products with ASE-GPC Coupled with Gas Chromatography

doi:10.7506/spkx1002-6630-200924078

FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (24): 351-354.doi: 10.7506/spkx1002-6630-200924078

Previous Articles Next Articles

Simultaneous Determination of 8 HCH and DDT Residues in Soybean and Soybean Products with ASE-GPC Coupled with Gas Chromatography

WEI Dong-xu1,2，JIANG Lian-zhou1,3,* GUO Wei1，MENG Bing-bing2，HU Shao-xin1

1. School of Food, Northeast Agricultural University, Harbin 150030, China；
2. Inspection and Quarantine Center, Heilongjiang Entry-Exit Inspection and Quarantine Bureau, Harbin 150001, China；
3. National Research Centre of Soybean Engineering and Technology, Harbin 150086, China

Received:2008-12-23 Revised:2009-08-13 Online:2009-12-15 Published:2010-12-29
Contact: JIANG Lian-zhou1,3,* E-mail:jlzname@163.com

Abstract

Abstract:

A method for the determination of 8 HCH and DDT in soybean and soybean products was established with accelerated solvent extraction (ASE), auto gel permeation chromatography purification (GPC) and gas chromatography quantification. The calibration curves presented good linear relationship in the range of 0.005－0.100 mg/kg, and the correlation coefficients were above 0.9990 for all compounds. Recoveries of all added were 78.3%－107.6% respectively, and relative standard deviations (RSD) were 2.1%－5.5% with spiked at 0.005, 0.020, 0.050 mg/kg of HCH and DDT in blank samples. The limit of detection of the method were 0.2 － 1.8μg/kg. The method was of good reproducibility, high sensitivity, shorter analysis time, and its performance could meet the requirements of the domestic and international legislation.

Key words: soybean and soybean products, accelerated solvent extraction (ASE), gel permeation chromatography (GPC), gas chromatography (GC), hexachlorocyclohexane (HCH), dichlorodiphenyl trichloroethane (DDT)

CLC Number:

TS207.53

WEI Dong-xu1,2，JIANG Lian-zhou1,3,* GUO Wei1，MENG Bing-bing2，HU Shao-xin1. Simultaneous Determination of 8 HCH and DDT Residues in Soybean and Soybean Products with ASE-GPC Coupled with Gas Chromatography[J]. FOOD SCIENCE, 2009, 30(24): 351-354.

[1]	HUANG Tiantian, TANG Hua, DONG Xiaoqian, LIU Songnan, XU Wenwen, WANG Hua, ZONG Qi. Determination of 23 Organophosphorus Pesticide Residues in Tea by QuEChERS Extraction with Multi-Walled Carbon Nanotubes (MWCNTs) Coupled to Gas Chromatography [J]. FOOD SCIENCE, 2018, 39(6): 315-321.
[2]	XIE Pujun, HUANG Lixin, ZHANG Caihong, DING Shasha, DENG Yejun, WANG Xiaojie. Characterization, Antioxidant Activity and Thermostabiltiy of Hydroxytyrosol Polymerization Products Catalyzed by Laccase [J]. FOOD SCIENCE, 2018, 39(16): 90-97.
[3]	LU Zhiyuan, ZHANG Yaowu, LI Xuejuan, FENG Xinyi, XUE Huihui, GUO Songnian, LIU Jia. Determination of β-Phenylethanol in Rice Wine by Solid Phase Extraction-Gas Chromatography [J]. FOOD SCIENCE, 2017, 38(24): 213-217.
[4]	DUAN Bing, HE Taixi, FAN Yuanyuan, ZHENG Bing. Determination of Imidacloprid and Acetamiprid in Tea by Gel Permeation ChromatographyUltra Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2016, 37(4): 238-241.
[5]	XU Renjie, CAI Chunping, DING Liping, LIN Jiaqing, CHEN Liye, FANG Ting, CHEN Jinquan. Simultaneous Determination of Hexachlorocyclohexanes, Dichlorodiphenyltrichloroethanes and Indicator Polychlorinated Biphenyls in Eggs and Egg Products by Double Depuration-Gas Chromatography [J]. FOOD SCIENCE, 2016, 37(24): 222-227.
[6]	WANG Meixia, ZHOU Dayun, MA Lei, XU Shuangjiao, WEI Shoujun, YANG Weihua, WANG Yanqin, DU Shuangkui,*. Analysis and Evaluation of Fatty Acid Composition in Cottonseed Oil [J]. FOOD SCIENCE, 2016, 37(22): 136-141.
[7]	CHEN Jianzhong, GE Shuilian, YANG Mingjian, ZHANG Yuan. Determination of Gardenia Yellow in Instant Noodle by Accelerated Solvent Extraction and High Performance Liquid Chromatography [J]. FOOD SCIENCE, 2016, 37(10): 208-212.
[8]	XU Mingya1, PAN Danjie1, JIN Micong2. Determination of Benzo(a) Pyrene in Edible Vegetable Oils by Gel Permeation Chromatography [J]. FOOD SCIENCE, 2015, 36(8): 240-243.
[9]	WANG Chen, LI Xiaoming, LU Yongling, ZHENG Tiesong, Lü Lishuang. Detection of Dicarbonyl Compounds in Beverages by Gas Chromatography [J]. FOOD SCIENCE, 2015, 36(24): 235-241.
[10]	ZHANG Wei, YANG Jianyuan, FAN Yawei, DENG Zeyuan. Optimization of Medium Composition for Soybean Hull Fiber Degradation by Neurospora crassa and Monosaccharide Composition Analysis of the Resulting Fermentable Sugars [J]. FOOD SCIENCE, 2015, 36(23): 209-214.
[11]	CAO Lili, CAO Xinmin, PANG Min, PAN Lijun, JIANG Shaotong*. Determination of Short and Long Chain Triglycerides in Edible Oils by Gas Chromatography [J]. FOOD SCIENCE, 2015, 36(2): 85-89.
[12]	ZHU Sai-feng, WU Jian-feng, ZHAO Xi-rong. Response Surface Methodology for Optimization of Culture Conditions for the Production of Tetramethylpyrazine by Bacillus subtilis S0507 [J]. FOOD SCIENCE, 2014, 35(9): 218-223.
[13]	ZHANG Quan, CHEN Wen-sheng*, HONG Liang, JIN Chun-jie, CHU Hong-chao. Simultaneous Determination of 8 Organochlorine Pesticide Residues in Chili Sauce by Gas Chromatography with Matrix Solid Phase Dispersion-Gel Permeation Chromatography Cleanup [J]. FOOD SCIENCE, 2014, 35(8): 295-298.
[14]	XING Li, GENG Yue*. Monosaccharide Component Analysis of Pea Flour Residue by Gas Chromatography [J]. FOOD SCIENCE, 2014, 35(22): 252-254.
[15]	WANG Ji-xiang, ZHANG Xue-zhong, WANG Ya-qin, NIU Zhi-rui, FENG Lei, ZHAO Yu. Uncertainty Evaluation for the Determination of Bifenthrin in Tea by Gas Chromatography and Gas Chromatography-Mass Spectrometry [J]. FOOD SCIENCE, 2014, 35(12): 200-203.

Simultaneous Determination of 8 HCH and DDT Residues in Soybean and Soybean Products with ASE-GPC Coupled with Gas Chromatography

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments