Determination of Sudan Pigment in Preserved Egg by Combination of Matrix Solid Phase Dispersion and High Performance Liquid Chromatography

FOOD SCIENCE ›› 2008, Vol. 29 ›› Issue (3): 400-402.

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Determination of Sudan Pigment in Preserved Egg by Combination of Matrix Solid Phase Dispersion and High Performance Liquid Chromatography

LIU Hong-Cheng, WANG Zhi-Fei, LI Qi-Wan, ZOU Yan-Hong, SHAO Jin-Liang, TANG Li-Bin

1.Supervision and Testing Center for Farm Product Quality, Ministry of Agriculture, Yunnan Academy of Agriculture Science, Kunming 650223, China;2.College of Chemistry and Biotechnology,Yunnan National University, Kunming 650091, China; 3.Kunming Institute of Physics, Kunming 650223, China

Online:2008-03-15 Published:2011-08-24

Abstract

Abstract: An analytic method for Sudan I～IV residues determination in preserved eggs by HPLC was developed. The sample was extracted and purified quickly by matrix solid phase dispersion (MSPD), separated by a Waters Nova-Park C18 (3.9mm×150 mm,5μm) and detected respectivey with two wavelengths UV detector at 478nm and 520 nm. Two pillars confirmed a positive result. The recoveries range of determination is 85.5%～97.5%. The relative standard deviation (RSD) is 3.1%～5.1%. The detection limit is 0.1μg/ml.

Key words: matrix solid phase dispersion, preserved egg, Sudan I～IV, HPLC

LIU Hong-Cheng, WANG Zhi-Fei, LI Qi-Wan, ZOU Yan-Hong, SHAO Jin-Liang, TANG Li-Bin. Determination of Sudan Pigment in Preserved Egg by Combination of Matrix Solid Phase Dispersion and High Performance Liquid Chromatography[J]. FOOD SCIENCE, 2008, 29(3): 400-402.

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Determination of Sudan Pigment in Preserved Egg by Combination of Matrix Solid Phase Dispersion and High Performance Liquid Chromatography

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