食品科学 ›› 2010, Vol. 31 ›› Issue (10): 263-267.doi: 10.7506/spkx1002-6630-201010057

• 分析检测 • 上一篇    下一篇

七种谷物麸皮中酚酸类成分分析

郝 杰,张长虹,曹学丽*   

  1. 北京工商大学化学与环境工程学院,北京市植物资源研究开发重点实验室
  • 收稿日期:2009-08-10 修回日期:2010-03-12 出版日期:2010-05-15 发布日期:2010-12-29
  • 通讯作者: 曹学丽 E-mail:crab_susu@yahoo.com.cn

RP-HPLC Analysis of Phenolic Acids in Different Varieties of Cereal Bran

HAO Jie,ZHANG Chang-hong,CAO Xue-li*   

  1. Beijing Key Laboratory of Plant Resources Research and Development, College of Chemical and Environmental Engineering,
    Beijing Technology and Business University, Beijing 100048, China
  • Received:2009-08-10 Revised:2010-03-12 Online:2010-05-15 Published:2010-12-29
  • Contact: CAO Xue-li E-mail:crab_susu@yahoo.com.cn

摘要:

利用反相高效液相色谱法(RP-HPLC)测定7 种不同种类及品种的谷物麸皮中8 种酚酸类成分的含量,并利用数学统计的方法对不同种类谷物、各类酚酸及总酚酸含量间的差异性进行分析。分析结果表明:所分析谷物种类所含酚酸的含量顺序为玉米>小麦>荞麦>燕麦,谷物麸皮中酚酸主要以束缚型酚酸形式存在,且肉桂酸类酚酸含量明显大于苯甲酸类酚酸,游离型及可溶共价结合型酚酸中4- 羟基苯甲酸、香草酸含量较高;而在束缚型酚酸中阿魏酸的含量在各类谷物中均最高,玉米品种中可达到6527.86μg/g 麸皮。

关键词: 谷物麸皮, 酚酸, 高效液相色谱

Abstract:

Eight phenolic acids (PAs) in different varieties of cereal bran including 3 wheat cultivars, 2 corn cultivars, 1 oat cultivar and 1 buckwheat cultivar were determined by the developed RP-HPLC method. Meanwhile, the differences in the contents of each PA and total PAs among the cereal bran materials were statistically analyzed. Results showed that the total PA contents in different varieties of cereal bran decreased in the following order: corn > wheat > buckwheat > oat. Bound PAs were the predominant PAs in the 4 varieties of cereal bran, of which, cinnamic acid exhibited a much higher content than benzoic acid. Of free and soluble covalent PAs, 4-hydroxybenzoic and vanilla acids both exhibited a higher content. Of bound PAs, the highest content of ferulic acid was observed in all the varieties of cereal bran and reached up to 6527.86 μg/g corn bran.

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