食品科学 ›› 2011, Vol. 32 ›› Issue (4): 223-226.doi: 10.7506/spkx1002-6630-201104050

• 分析检测 • 上一篇    下一篇

食品接触塑料制品中高锰酸钾消耗量测定不确定度分析

曹国洲,袁巍巍,李 绿,刘在美,孙 斌   

  1. 宁波出入境检验检疫局
  • 出版日期:2011-03-12 发布日期:2017-04-06

Evaluation of Measurement Uncertainty for the Determination of Potassium Permanganate Consumption of Food Contact Plastics

CAO Guo-zhou,YUAN Wei-wei,LI Lu,LIU Zai-mei,SUN Bin   

  1. Ningbo Entry-exit Inspection and Quarantine Bureau, Ningbo 315012, China
  • Online:2011-03-12 Published:2017-04-06

摘要: 对于GB/T 5009.60-2003《食品包装用聚乙烯、聚苯乙烯、聚丙烯成型品卫生标准的分析方法》测定食品接触塑料制品高锰酸钾消耗量,分析其测定过程的影响因素,归纳出不确定度的主要来源,形成不确定度评定程序和方法,经量化和合成得到相对标准不确定度,从而求得扩展不确定度。即当高锰酸钾消耗量为2.26mg/L时,相对标准不确定度为0.039,扩展不确定度为0.176mg/L(k=2)。

关键词: 塑料制品, 高锰酸钾消耗量, 不确定度

Abstract: In this study, factors affecting the determination of KMnO4 consumption of food contact plastics by the method of the Chinese National Standard GB/T 5009-2003 were analyzed, the main sources of measurement certainty were summarized, a procedure for certainty evaluation was established, and a relative standard uncertainty was obtained after calculating and synthesizing various uncertainty components and expanded. Potassium permanganate consumption was determined to be 2.26 mg/L for a polyethylene food box from a certain manufacturer, and the relative standard uncertainty for the determination was 0.039, and the expanded uncertainty was 0.176 mg/L (k = 2).

Key words: plastic articles, KMnO4 consumption, uncertainty

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